HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminobenzoic Acid → HCID 56942027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminobenzoic Acid | HCID 7419 | — |
| Reactant | 5-Methoxy-3-methylbenzothiophene-2-sulfonyl chloride | HCID 57440339 | — |
| Product | HCID 56942027 | HCID 56942027 | 33% |
Reaction Steps
The product was prepared according to General Procedure 1, described in Example 1, with 5-methoxy-3-methylbenzothiophene-2-sulfonyl chloride (Intermediate 8) (85 mg, 0.31 mmol) and 3-aminobenzoic acid (42 mg, 0.31 mmol). The title compound was obtained in 33% yield (38.2 mg). MS (ESI+) calcd mass for C17H15NO5S2 377.039164, found 377.039474.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-2691e0699bfa49f5aa4424d3c3d5854d |
| Source note | uspto-grants-2016_01 |