3-Aminobenzoic Acid → HCID 56942028, compound

HRID 589749Notes

Reaction equation

HRID 589749 reaction equation
[C:1]1([C:7]2[CH:8]=[C:9]([S:13](Cl)(=[O:15])=[O:14])[CH:10]=[CH:11][CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[NH2:17][C:18]1[CH:19]=[C:20]([CH:24]=[CH:25][CH:26]=1)[C:21]([OH:23])=[O:22]>>[C:7]1([C:1]2[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=2)[CH:12]=[CH:11][CH:10]=[C:9]([S:13]([NH:17][C:18]2[CH:19]=[C:20]([CH:24]=[CH:25][CH:26]=2)[C:21]([OH:23])=[O:22])(=[O:15])=[O:14])[CH:8]=1

Participants

3

Reactant 2

HCID 74193-Aminobenzoic AcidHCID 38027523-Phenylbenzene-1-sulfonyl chloride

Product 1

HCID 56942028HCID 56942028, compoundYield 100%

Procedure

The product was prepared according to General Procedure 1, described in Example 1, with 3-phenylbenzenesulfonylchloride (13.9 mg, 0.055 mmol) and 3-aminobenzoic acid (6.9 mg, 0.050 mmol). The title compound was obtained in 100% yield (17.7 mg). MS (ESI+) calcd mass for C19H15NO4S 353.072179, found 353.071899.

Workup

  1. customThe product was prepared

Sources & evidence

ORD record
ord-7dbe64bf98df426b9d84c6c424dd59b3
Source dataset
uspto-grants-2016_01
Patent number
US09233946B2

Reaction notes

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