HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzothiophene-2-sulfonyl chloride → HCID 178527475, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzothiophene-2-sulfonyl chloride | HCID 2776333 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | HCID 178527475 | HCID 178527475 | 60% |
Reaction Steps
The product was prepared according to General Procedure 1, described in Example 1, with 1-benzothiophene-2-sulfonyl chloride (12.8 mg, 0.055 mmol) and 5-(3-amino-phenyl)tetrazole (8.0 mg, 0.050 mmol). The title compound was obtained in 60% yield (10.8 mg). MS (ESI+) calcd mass for C15H11N5O2S2 357.035416, found 357.036256.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-8d7424a95518459c8c92aac0d6afe424 |
| Source note | uspto-grants-2016_01 |