HuagongsheHuagongshe Chemistry Print Report · For research reference only
4'-Methoxybiphenyl-4-sulfonyl chloride → 4'-Methoxy-N-[3-(1H-tetrazol-5-yl)phenyl]biphenyl-4-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4'-Methoxybiphenyl-4-sulfonyl chloride | HCID 2794750 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | 4'-Methoxy-N-[3-(1H-tetrazol-5-yl)phenyl]biphenyl-4-sulfonamide | HCID 178488633 | 79% |
Reaction Steps
The product was prepared according to General Procedure 1, described in Example 1, with 4′-methoxy[1,1′-biphenyl]-4-sulfonyl chloride (15.6 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8.0 mg, 0.050 mmol). The title compound was obtained in 79% yield (16 mg). MS (ESI+) calcd mass for C20H17N5O3S 407.105210, found 407.105280.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-b1795f03a6ae48cf813d6967030468e0 |
| Source note | uspto-grants-2016_01 |