Benzoic acid, 3-amino-, methyl ester → HCID 66802143, compound

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Reaction Steps

The title compound was prepared according to General Procedure 1, described in Example 1, with 5-(2-methylthiazol-4-yl)thiophene-2-sulphonylchloride (15.4 mg, 0.055 mmol) and methyl 3-aminobenzoate (7.6 mg, 0.050 mmol). 1H NMR (400 MHz, DMSO-d6) δ ppm 1.82-1.83 (s, 3H), 2.98-2.99 (s, 3H), 6.59-6.62 (m, 2H), 6.67-6.68 (s, 2H), 6.81-6.84 (m, 1H), 6.93-6.94 (m, 1H). MS (ESI+) m/z 395 [M+H]+.

Provenance & Evidence