HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichlorobenzeneboronic acid → HCID 178527487, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichlorobenzeneboronic acid | HCID 2734330 | — |
| Reactant | HCID 178527479 | HCID 178527479 | — |
| Product | HCID 178527487 | HCID 178527487 | 4% |
Reaction Steps
The product was prepared according to General Procedure 3, described in Example 22, using 5-bromo-N-[3-(1H-tetrazol-5-yl)phenyl]thiophene-2-sulfonamide (Intermediate 17) (19 mg, 0.055 mmol) and 3,4-dichlorophenylboronic acid (11 mg, 0.06 mmol). The title compound was obtained in 4% yield (0.8 mg). MS (ESI+) m/z 452 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-d7fb0060553541f48f7412ede8b0ddff |
| Source note | uspto-grants-2016_01 |