HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Aminosalicylic Acid → HCID 66799893, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Aminosalicylic Acid | HCID 4075 | — |
| Reactant | 3-(4-chlorophenyl)benzenesulfonyl Chloride | HCID 3502760 | — |
| Product | HCID 66799893 | HCID 66799893 | 33% |
Reaction Steps
The product was prepared according to General Procedure 1, described in Example 1, with [[3-(4-chlorophenyl)phenyl]sulfonyl chloride (16 mg, 0.055 mmol) and 5-aminosalicylic acid (7.7 mg, 0.050 mmol) using a modified reaction temperature of 60° C. The title compound was obtained in 33% yield (6.7 mg). MS (ESI+) calcd mass for C19H14ClNO5S 403.028121, found 403.028561.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-571715aa18bf4489b09f51a222271d99 |
| Source note | uspto-grants-2016_01 |