HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(Phenylsulfonyl)-2-thiophenesulfonyl chloride → HCID 178527510, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(Phenylsulfonyl)-2-thiophenesulfonyl chloride | HCID 580877 | — |
| Reactant | HCID 178507542 | HCID 178507542 | — |
| Product | HCID 178527510 | HCID 178527510 | 40% |
Reaction Steps
The product was prepared according to General Procedure 1, described in Example 1, with 5-benzenesulfonyl-thiophene-2-sulfonyl chloride (17.7 mg, 0.055 mmol) and 5-(3-aminophenyl)tetrazole (8.0 mg, 0.050 mmol). The title compound was obtained in 40% yield (8.9 mg). MS (ESI+) calcd mass for C17H13N5O4S3 447.012966, found 447.013676.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233946B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-78ae26d1a32d47cfa5d747cd3a95730a |
| Source note | uspto-grants-2016_01 |