Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sulfamide | HCID 82267 | — |
| Reactant | 3-Oxetanamine | HCID 9833923 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86706429 | HCID 86706429 | — |
Reaction Steps
Sulfamide (15.6 mmol) was dissolved in H2O (8 mL), added oxetan-3-amine (6.85 mmol) and stirred at 70° C. for 16 h and then at 100° C. for another 16 h. The obtained reaction mixture was cooled to rt and freezedried affording the title compound as white solid. Used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09233964B2 |
|---|
| Source dataset | uspto-grants-2016_01 |
|---|
| ORD ID | ord-6d57d27b869749ca87c44d3f7a808df6 |
|---|
| Source note | uspto-grants-2016_01 |
|---|
