Sulfamide → HCID 86706429, compound

HRID 589956Notes

Reaction equation

HRID 589956 reaction equation
[S:1]([NH2:5])([NH2:4])(=[O:3])=[O:2].[O:6]1[CH2:9][CH:8](N)[CH2:7]1>O>[S:1]([NH:5][CH:8]1[CH2:9][O:6][CH2:7]1)(=[O:3])(=[O:2])[NH2:4]

Participants

4

Reactant 2

HCID 82267SulfamideHCID 98339233-Oxetanamine

Product 1

HCID 86706429HCID 86706429, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
70 °C

Procedure

Sulfamide (15.6 mmol) was dissolved in H2O (8 mL), added oxetan-3-amine (6.85 mmol) and stirred at 70° C. for 16 h and then at 100° C. for another 16 h. The obtained reaction mixture was cooled to rt and freezedried affording the title compound as white solid. Used without further purification.

Workup

  1. waitat 100° C. for another 16 h
  2. customThe obtained reaction mixture
  3. temperaturewas cooled to rt
  4. customfreezedried

Sources & evidence

ORD record
ord-6d57d27b869749ca87c44d3f7a808df6
Source dataset
uspto-grants-2016_01
Patent number
US09233964B2

Reaction notes

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