HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfamide → HCID 86706430, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfamide | HCID 82267 | — |
| Reactant | 3-(Aminomethyl)-1lambda~6~-thiolane-1,1-dione | HCID 2772225 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86706430 | HCID 86706430 | — |
Reaction Steps
Sulfamide (2.4 mmol) was dissolved in H2O (10 mL), added (1,1-dioxothiolan-3-yl)methanamine (2 mmol) and stirred at reflux for 16 h. The obtained reaction mixture was cooled to rt and freezedried affording the title compound as an oil. Used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233964B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-bc55470bd0764475824846dcf93f7959 |
| Source note | uspto-grants-2016_01 |