Sulfamide → HCID 86706430, compound

HRID 589957Notes

Reaction equation

HRID 589957 reaction equation
[S:1]([NH2:5])([NH2:4])(=[O:3])=[O:2].[O:6]=[S:7]1(=[O:14])[CH2:11][CH2:10][CH:9]([CH2:12]N)[CH2:8]1>O>[O:6]=[S:7]1(=[O:14])[CH2:11][CH2:10][CH:9]([CH2:12][NH:4][S:1](=[O:3])(=[O:2])[NH2:5])[CH2:8]1

Participants

4

Reactant 2

HCID 82267SulfamideHCID 27722253-(Aminomethyl)-1lambda~6~-thiolane-1,1-dione

Product 1

HCID 86706430HCID 86706430, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Sulfamide (2.4 mmol) was dissolved in H2O (10 mL), added (1,1-dioxothiolan-3-yl)methanamine (2 mmol) and stirred at reflux for 16 h. The obtained reaction mixture was cooled to rt and freezedried affording the title compound as an oil. Used without further purification.

Workup

  1. temperatureat reflux for 16 h
  2. customThe obtained reaction mixture
  3. customfreezedried

Sources & evidence

ORD record
ord-bc55470bd0764475824846dcf93f7959
Source dataset
uspto-grants-2016_01
Patent number
US09233964B2

Reaction notes

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