HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 590533Generated: October 26, 2026
Methyl Acrylate → HCID 131734482, compound
https://huagongshe.com/reaction/590533
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl Acrylate | HCID 7294 | — |
| Reactant | Tert-butyl-dimethyl-piperazin-1-ylsilane | HCID 19434780 | — |
| Product | HCID 131734482 | HCID 131734482 | — |
Reaction Steps
A flask equipped with a stirrer, reflux condenser, dropping funnel and thermometer was charged with 160.3 g (0.8 mol) of 1-t-butyldimethylsilylpiperazine (Synthesis Example 1) and heated at 70° C. Once the internal temperature became steady, 75.8 g (0.88 mol) of methyl acrylate was added dropwise over 2 hours. Stirring was continued for 4 hours at the temperature. On distillation of the reaction solution, 219.9 g of a fraction having a boiling point of 135-137° C./0.4 kPa was collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09233988B2 |
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| Source dataset | uspto-grants-2016_01 |
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| ORD ID | ord-61dd056323314b5291c3f737c6851283 |
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| Source note | uspto-grants-2016_01 |
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