Methyl Acrylate → HCID 131734485, compound

Participants

Reaction Conditions

Reaction Steps

A flask equipped with a stirrer, reflux condenser, dropping funnel and thermometer was charged with 194.0 g (0.8 mol) of 1-triisopropylsilylpiperazine (Synthesis Example 2) and heated at 70° C. Once the internal temperature became steady, 75.8 g (0.88 mol) of methyl acrylate was added dropwise over 2 hours. Stirring was continued for 4 hours at the temperature. On distillation of the reaction solution, 250.0 g of a fraction having a boiling point of 163-164° C./0.4 kPa was collected.

Provenance & Evidence