HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ruthenium trichloride → HCID 86694788, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ruthenium trichloride | HCID 61850 | — |
| Reactant | HCID 86694789 | HCID 86694789 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86694788 | HCID 86694788 | — |
Reaction Steps
The reaction product mixture containing dihydride biphenyl is made to contact ruthenium chloride in ethanol, wherein, amount of the reaction product mixture containing dihydride biphenyl should be such that the molar ratio of dihydride biphenyl to ruthenium chloride is 5:1, the contacting temperature is 80° C., the contacting time is 8 hours. On the basis that the total weight of dihydride biphenyl and ruthenium chloride is 100 mg, 60 ml of ethanol should be used. The mixture is filtered and washed with methanol to obtain biphenyl ruthenium trichloride dimer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09233995B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-e53f8d8e89ad4bf99e06c29a76e92d49 |
| Source note | uspto-grants-2016_01 |