HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Chloropicolinic acid → N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-6-chloropicoline amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Chloropicolinic acid | HCID 20812 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 6-chloropyridine-2-carbonyl Chloride | HCID 10942976 | — |
| Reactant | 2-Bromo-4-(1,2,2,2-tetrafluoro-1-(trifluoromethyl)ethyl)-6-(trifluoromethyl)benzenamine | HCID 58297558 | — |
| Product | N-(2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-6-chloropicoline amide | HCID 86654246 | — |
Reaction Steps
According to the method of 1-3 of Example 1, a target compound was prepared from 2-chloropyridine-6-carboxylic acid chloride prepared from 2-chloropyridine-6-carboxylic acid and thionyl chloride, and 2-bromo-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)aniline obtained in 1-2 of Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09237745B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-d3e8011c0ff54b32a1ab50774b349f6f |
| Source note | uspto-grants-2016_01 |