HRID591186

反应详情

EQUATION

反应方程式

HRID 591186 反应方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

(3-Benzyloxy-phenyl)-[1-(4-chloro-phenyl)-cyclobutyl]-methanone (780 mg, 2 mmol) was dissolved in ethyl acetate, containing Pd/C (80 mg, 10% on C). Hydrogenation was performed at room temperature during 4 hours. Reaction was filtered through celite and the solvent evaporated. The product (548 mg) was used in the next step without further purification.

WORKUP

后处理

  1. customReaction
  2. filtrationwas filtered through celite
  3. customthe solvent evaporated
  4. customThe product (548 mg) was used in the next step without further purification