Sodium ethoxide → HCID 51347689, compound

Participants

Reaction Conditions

Reaction Steps

Intermediate 12 (0.29 g, 0.712 mmol) was added to sodium ethoxide (ALDRICH, 0.145 g, 2.136 mmol) in ethanol (5 mL). The mixture was heated under microwave irradiation at 120° C. for 30 minutes. Solvent was removed under vacuum and the crude mixture was purified by flash chromatography (Si, eluting Hexane/EtOAc mixtures from 90:10 to 0:100%) to yield the title compound as a white solid.

Provenance & Evidence