Sodium ethoxide → HCID 51347690, compound

Participants

Reaction Conditions

Reaction Steps

Intermediate 14 (0.19 g, 0.488 mmol) was added to sodium ethoxide (ALDRICH, 0.1 g, 1.464 mmol) in ethanol (4 mL). The mixture was heated under microwave irradiation at 120° C. for 30 minutes and solvent was removed under vacuum to yield a yellowish residue. The crude mixture was purified by flash chromatography (Si, eluting with Hexane/EtOAc mixtures from 90:10 to 0:100%) to yield the title compound as a white solid.

Provenance & Evidence