反应详情

To a solution of 4-[3-(benzyloxy)propyl]benzaldehyde (1.86 g, 7.31 mmol) in ethanol (28 mL), sodium borohydride (83 mg, 2.19 mmol) was slowly added at room temperature. The mixture was stirred for 1 h. Water (50 mL) was added, and the mixture was extracted with ethyl acetate (3×50 mL), dried over magnesium sulfate and concentrated in vacuo. The crude product was used without purification.

1. extractionthe mixture was extracted with ethyl acetate (3×50 mL)
2. dry with materialdried over magnesium sulfate
3. concentrationconcentrated in vacuo
4. customThe crude product was used without purification