HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 69135266, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 57431992 | HCID 57431992 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69135266 | HCID 69135266 | — |
Reaction Steps
To a solution of 4-[3-(benzyloxy)propyl]benzaldehyde (1.86 g, 7.31 mmol) in ethanol (28 mL), sodium borohydride (83 mg, 2.19 mmol) was slowly added at room temperature. The mixture was stirred for 1 h. Water (50 mL) was added, and the mixture was extracted with ethyl acetate (3×50 mL), dried over magnesium sulfate and concentrated in vacuo. The crude product was used without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09238631B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-730efe2c226d4ce9b20d03f1c8ddbff0 |
| Source note | uspto-grants-2016_01 |