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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 591264Generated: October 30, 2026

Water → HCID 69135266, compound

https://huagongshe.com/reaction/591264

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantSodium borohydrideHCID 4311764—
ReactantHCID 57431992HCID 57431992—
SolventEthanolHCID 702—
ProductHCID 69135266HCID 69135266—

Reaction Steps

To a solution of 4-[3-(benzyloxy)propyl]benzaldehyde (1.86 g, 7.31 mmol) in ethanol (28 mL), sodium borohydride (83 mg, 2.19 mmol) was slowly added at room temperature. The mixture was stirred for 1 h. Water (50 mL) was added, and the mixture was extracted with ethyl acetate (3×50 mL), dried over magnesium sulfate and concentrated in vacuo. The crude product was used without purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09238631B2
Source datasetuspto-grants-2016_01
ORD IDord-730efe2c226d4ce9b20d03f1c8ddbff0
Source noteuspto-grants-2016_01