HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 89775320, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 118667063 | HCID 118667063 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 89775320 | HCID 89775320 | 88.6% |
Reaction Steps
To a mixture of methyl(7-acetyl-6-((2,4-dichlorobenzyl)oxy)-1-benzofuran-3-yl)acetate (100 mg) in MeOH (2.5 mL) was added NaBH4 (10.2 mg). The mixture was stirred at room temperature for 20 min. The mixture was quenched with water. The resulting solid was collected by filtration to give the title compound (89 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09238639B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-b71c184961d941b08666dd3191ae9f7a |
| Source note | uspto-grants-2016_01 |