HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethyl-3-(3'-dimethylaminopropyl)carbodiimide → HCID 118656288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethyl-3-(3'-dimethylaminopropyl)carbodiimide | HCID 15908 | — |
| Reactant | Methanesulfonamide | HCID 72879 | — |
| Reactant | HCID 118656238 | HCID 118656238 | — |
| Catalyst | 4-(Dimethylamino)pyridine | HCID 14284 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 118656288 | HCID 118656288 | — |
Reaction Steps
To a mixture of 6-((2,4-dichlorobenzyl)oxy)-2,3-dihydro-1-benzofuran-3-carboxylic acid (120 mg) in DMF (dry) (3.5 mL) were added methanesulfonamide (101 mg), EDCI (203 mg) and DMAP (130 mg). The mixture was stirred at room temperature overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09238639B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-1e7a4204417247bd8643484ef4ad5cab |
| Source note | uspto-grants-2016_01 |