HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Acetate → HCID 131734533, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Acetate | HCID 517045 | — |
| Reactant | O-Methylhydroxylamine hydrochloride | HCID 521874 | — |
| Reactant | HCID 46299459 | HCID 46299459 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 131734533 | HCID 131734533 | 56.7% |
Reaction Steps
To a mixture of 6-(2,4-dichlorobenzyloxy)benzofuran-3(2H)-one (2.0 g) in MeOH (20 mL) were added sodium acetate (0.531 g) and O-methylhydroxylamine hydrochloride (0.540 g). The mixture was refluxed overnight. After cooling, the mixture was concentrated. The residue was washed with water and EtOAc to give the title compound (1.24 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09238639B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-4c8a0577c9b64a75967872df27ddf4bc |
| Source note | uspto-grants-2016_01 |