HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 89768032, compound → HCID 89767861, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 89768032 | HCID 89768032 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 89767861 | HCID 89767861 | 96.4% |
Reaction Steps
To a mixture of methyl 3-hydroxy-2-(6-((4-methoxybenzyl)oxy)-1-benzofuran-3-yl)propanoate (86.9 mg) and MeOH (2.4 mL) was added 10% palladium on carbon (15 mg). The mixture was hydrogenated under balloon pressure for 21 h. The catalyst was removed by filtration and concentrated to give the title compound (56.0 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09238639B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-0215ecaf60804880a6e1852dd01a4c52 |
| Source note | uspto-grants-2016_01 |