Methanol → HCID 89725567, compound

Participants

Reaction Steps

To a solution of compound 39 (200 mg, 0.75 mmol) in MeOH (2 ml) was added NaOH (120 mg, 3.01 mmol). The reaction mixture was stirred at r.t ° C. for 4 h. checked TLC, starting material consumed, adjust the pH up to 6 using 50% HCl and concentrated under vacuum to obtain 178 mg (100%) a white solid.

Provenance & Evidence