HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Formylbenzoic acid → Ethyl 2-(4-formylbenzamido)-3-hydroxypropanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Formylbenzoic acid | HCID 12088 | — |
| Reactant | Ethyl 2-amino-3-hydroxypropanoate | HCID 410488 | — |
| Product | Ethyl 2-(4-formylbenzamido)-3-hydroxypropanoate | HCID 89725943 | 34% |
Reaction Steps
In an analogous manner to 39, 4-formyl benzoic acid (24) (1.0 g, 6.66 mmol) and ethyl 2-amino-3-hydroxypropanoate (975 mg, 7.33 mmol) were reacted to yield 600 mg (34%) of 41 as an off-white sticky solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09238656B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-e422a4522b1845cb85bf71cc7875e3ee |
| Source note | uspto-grants-2016_01 |