HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-(4-formylphenoxy)acetate → Acetic acid, 2-(4-formylphenoxy)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-(4-formylphenoxy)acetate | HCID 291358 | — |
| Reactant | 2-(3-Formylphenoxy)acetic acid | HCID 601895 | — |
| Product | Acetic acid, 2-(4-formylphenoxy)- | HCID 89177 | 57% |
Reaction Steps
Ethyl 2-(4-formylphenoxy)acetate (52) was treated in an analogous manner to compound 48 to yield the desired product (57%) as a white solid. NMR: δ 4.834 (s, 2H), 7.112 (d, J=7.2 Hz, 2H), 7.866 (d, J=7.6 Hz, 2H), 9.878 (s, 1H), 13.146 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09238656B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-d2b3ba8f4f444c928787ce77a5c9bf23 |
| Source note | uspto-grants-2016_01 |