HCID 66690551, compound → HCID 66690544, compound

Participants

Reaction Steps

The solution of methyl 4′-fluoro-6-hydroxy-5-nitrobiphenyl-3-carboxylate (13.0 mg, 45.0 μmol) and palladium (10% on carbon; 4.75 mg, 4.46 μmol) in ethanol (5 mL) was degassed and stirred under hydrogen at 1 atm. After 1 h, the mixture was filtered and washed with ethanol. The filtrate was concentrated to dryness to give the title compound (10 mg). LC-MS [M+1]=262.1.

Provenance & Evidence