HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dichlorobenzamide → 2,6-Dichlorobenzoyl isocyanate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dichlorobenzamide | HCID 16183 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 2,6-Dichlorobenzoyl isocyanate | HCID 12912739 | 88% |
Reaction Steps
The title compound was prepared according to the procedure described in step-2 of Intermediate-8 by using 2,6-dichlorobenzamide (1.00 g, 5.26 mmol), oxalyl chloride (0.795 g, 6.31 mmol) and toluene (10 mL) to afford 1.00 g of desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09439890B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-5fca01153ddf4ee394514e15cea7298b |
| Source note | uspto-grants-2016_09 |