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HRID592602

反应详情

EQUATION

反应方程式

HRID 592602 的结构方程式

REACTANTS

反应物

3
结构：O=[N+]([O-])c1ccc(Br)cn1
HCID817620

5-Bromo-2-nitropyridine

C5H3BrN2O2

结构：CC(C)(C)OC(=O)N1CCN(c2ccc([N+](=O)[O-])nc2)CC1
HCID11243758

Tert-butyl 4-(6-nitropyridin-3-yl)piperazine-1-carboxylate

C14H20N4O4

结构：C[C@@H]1CN[C@@H](C)CN1C(=O)OC(C)(C)C
HCID24903576

未命名化合物

PRODUCTS

生成物

1
结构：C[C@@H]1CN(c2ccc([N+](=O)[O-])nc2)[C@@H](C)CN1C(=O)OC(C)(C)C
HCID86683703

未命名化合物

收率 75%

PROCEDURE

实验过程

Following the procedures as described for compound 101g, (2R,5S)-tert-butyl-2,5-dimethylpiperazine-1-carboxylate (1.5 g, 6.0 mmol), and 5-bromo-2-nitropyridine (1212 mg, 6.0 mmol) were reacted to give 122a as a yellow solid (1500 mg, 75%). LCMS: [M+H]+ 337

WORKUP

后处理

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