HCID 131734558, compound → Calcium di(L-lysinate)

Participants

Reaction Steps

A stirred solution of calcium bis-lysinate monohydrate (1.92 g, 5.0 mmol) in methanol (10 mL) was treated with a solution of EPA (1.55 g, 5.125 mmol) in methanol (10 mL) and stirred for 15 min, then concentrated in vacuo to a pale yellow foam. The above foam was triturated from acetonitrile (20 mL) and dried in vacuo to afford 3.26 g (97%) of subject material as a pale yellow powder.

Provenance & Evidence