Thionyl Chloride → HCID 63428983, compound

Participants

Reaction Steps

To a solution of (3-iodophenyl)-p-tolylmethanol (2.68 g) in dichloromethane (50 mL) at 0° C. is slowly added thionyl chloride (633 μL). After stirring at room temperature for 2 days, the mixture is washed with aqueous NaHCO3, dried over magnesium sulfate and concentrated under reduced pressure to afford chloro-(3-iodophenyl)-p-tolylmethane.

Provenance & Evidence