HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyridazinamine, 6-ethoxy- → HCID 89876019, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyridazinamine, 6-ethoxy- | HCID 3084748 | — |
| Reactant | 4-((3,5-Dimethylisoxazol-4-yl)methoxy)benzene-1-sulfonyl chloride | HCID 16490702 | — |
| Product | HCID 89876019 | HCID 89876019 | 4% |
Reaction Steps
The title compound (16 mg) was prepared from 6-ethoxypyridazin-3-amine (129 mg, 1.0 mmol) and 4-{[(3,5-dimethyl-4-isoxazolyl)methyl]oxy}benzenesulfonyl chloride (0.302 g, 1.0 mmol), following the procedure described for Intermediate 51. LCMS (2 min, formic) Rt 0.91 min, m/z (ES+) 405 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242972B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-726b1d7101dd43029f93e1a292dea8a8 |
| Source note | uspto-grants-2016_01 |