HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 61147895, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 61147515 | HCID 61147515 | — |
| Catalyst | HCID 178503042 | HCID 178503042 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 61147895 | HCID 61147895 | 101% |
Reaction Steps
Under an argon atmosphere, to a solution of 2-(4-bromophenoxy)-5-nitropyrimidine (400 mg) in tetrahydrofuran (20 mL)/methanol (20 mL) was added 3% platinum-carbon (200 mg). The reaction mixture was stirred under a hydrogen atmosphere at room temperature for 3 hours. The reaction mixture was filtered through Celite® to give the titled compound (363 mg) having the following physical data.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242977B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-f367567c98684bd99758d6ed22449b00 |
| Source note | uspto-grants-2016_01 |