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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 594199Generated: November 2, 2026

Methanol → HCID 61147895, compound

https://huagongshe.com/reaction/594199

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 61147515HCID 61147515—
CatalystHCID 178503042HCID 178503042—
SolventTetrahydrofuranHCID 8028—
ProductHCID 61147895HCID 61147895101%

Reaction Steps

Under an argon atmosphere, to a solution of 2-(4-bromophenoxy)-5-nitropyrimidine (400 mg) in tetrahydrofuran (20 mL)/methanol (20 mL) was added 3% platinum-carbon (200 mg). The reaction mixture was stirred under a hydrogen atmosphere at room temperature for 3 hours. The reaction mixture was filtered through Celite® to give the titled compound (363 mg) having the following physical data.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09242977B2
Source datasetuspto-grants-2016_01
ORD IDord-f367567c98684bd99758d6ed22449b00
Source noteuspto-grants-2016_01