huagongshe.com
HRID594456

反应详情

EQUATION

反应方程式

HRID 594456 的结构方程式

REACTANTS

反应物

2
结构：O=Cc1cccc(-c2ccccn2)n1
HCID11095276

[2,2'-Bipyridine]-6-carbaldehyde

C11H8N2O

结构：COC(=O)CCCC(N)c1c(OC)cccc1OC
HCID69082713

未命名化合物

PRODUCTS

生成物

1
结构：COc1cccc(OC)c1C1CCCC(=O)N1Cc1cccc(-c2ccccn2)n1
HCID69085730

未命名化合物

PROCEDURE

实验过程

Prepared according to the described general procedure 1 (GP1) by reaction of methyl 5-amino-5-(2,6-dimethoxyphenyl)pentanoate with [2,2′-bipyridine]-6-carbaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.58 min.; [M+H]+: 403.99 g/mol.

WORKUP

后处理

  1. customPrepared
  2. customSubsequent purification by preparative HPLC
  3. customafforded the target compound