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HRID594595

反应详情

EQUATION

反应方程式

HRID 594595 的结构方程式

REACTANTS

反应物

2
结构：COc1cccc(OC)c1C1CCCC(=O)N1
HCID69082526

未命名化合物

结构：FC(F)Oc1ccc(CBr)cn1
HCID69085387

5-(Bromomethyl)-2-(difluoromethoxy)pyridine

C7H6BrF2NO

PRODUCTS

生成物

1
结构：COc1cccc(OC)c1C1CCCC(=O)N1Cc1ccc(OC(F)F)nc1
HCID69082715

未命名化合物

PROCEDURE

实验过程

Prepared according to the described general procedure 4 (GP4) by reaction of 6-(2,6-dimethoxyphenyl)piperidin-2-one with 5-(bromomethyl)-2-(difluoromethoxy)pyridine. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions D): tR=1.03 min.; [M+H]+: 393.53 g/mol.

WORKUP

后处理

  1. customPrepared
  2. customSubsequent purification by preparative HPLC
  3. customafforded the target compound