huagongshe.com
HRID594613

反应详情

EQUATION

反应方程式

HRID 594613 的结构方程式

REACTANTS

反应物

2
结构：FC(F)(F)Oc1ccc(CBr)cc1
HCID142785

4-(Trifluoromethoxy)benzyl bromide

C8H6BrF3O

结构：CCOc1ccccc1C1CCC(=O)N1
HCID69082481

未命名化合物

PRODUCTS

生成物

1
结构：CCOc1ccccc1C1CCC(=O)N1Cc1ccc(OC(F)(F)F)cc1
HCID69083688

未命名化合物

PROCEDURE

实验过程

Prepared according to the described general procedure 4 (GP4) by reaction of 5-(2-ethoxyphenyl)pyrrolidin-2-one with commercially available 1-(bromomethyl)-4-(trifluoromethoxy)benzene. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions D): tR=1.08 min.; [M+H]+: 379.99 g/mol.

WORKUP

后处理

  1. customPrepared
  2. customSubsequent purification by preparative HPLC
  3. customafforded the target compound