HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoethyl methyl ether → HCID 69084618, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoethyl methyl ether | HCID 80972 | — |
| Reactant | HCID 69083694 | HCID 69083694 | — |
| Product | HCID 69084618 | HCID 69084618 | — |
Reaction Steps
Prepared according to the described general procedure 7 (GP7) by O-alkylation of 6-(2-hydroxy-6-methoxyphenyl)-1-(4-(trifluoromethoxy)benzyl)piperidin-2-one with commercially available 1-bromo-2-methoxyethane. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions E): tR=0.80 min.; [M+H]+: 454.25 g/mol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242970B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-6d9fd63eb0524c0ba78fb74ea8c2c5fa |
| Source note | uspto-grants-2016_01 |