HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dimethoxybenzaldehyde → 6-(2,6-dimethoxyphenyl)-1-((1-methyl-1H-benzo[d][1,2,3]triazol-5-yl)methyl)piperidin-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dimethoxybenzaldehyde | HCID 96404 | — |
| Reactant | (1-Methyl-1H-1,2,3-Benzotriazol-5-Yl)Methylamine | HCID 2795420 | — |
| Product | 6-(2,6-dimethoxyphenyl)-1-((1-methyl-1H-benzo[d][1,2,3]triazol-5-yl)methyl)piperidin-2-one | HCID 86695653 | — |
Reaction Steps
Prepared according to the described general procedure 6 (GP6) with commercially available (1-methyl-1H-benzo[d][1,2,3]triazol-5-yl)methanamine and commercially available 2,6-dimethoxybenzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions E): tR=0.65 min.; [M+H]+: 381.09 g/mol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242970B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-b59890ace319484fa4eae81eebbfca35 |
| Source note | uspto-grants-2016_01 |