HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(Trifluoromethoxy)phenylboronic Acid (contains varying amounts of Anhydride) → HCID 86695654, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(Trifluoromethoxy)phenylboronic Acid (contains varying amounts of Anhydride) | HCID 2777204 | — |
| Reactant | HCID 69083750 | HCID 69083750 | — |
| Product | HCID 86695654 | HCID 86695654 | — |
Reaction Steps
Prepared according to the described general procedure 9 (GP9) with 6-oxo-1-(4-(trifluoromethoxy)benzyl)-1,4,5,6-tetrahydropyridin-2-yl diphenyl phosphate and commercially available (2-(trifluoromethoxy)phenyl)boronic acid. Subsequent hydrogenation and purification by preparative HPLC afforded the target compound. LC-MS (conditions E): tR=0.83 min.; [M+H]+: 433.70 g/mol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242970B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-1a6271c61e5346e2aaa6bf7617018d9e |
| Source note | uspto-grants-2016_01 |