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HRID594678

反应详情

EQUATION

反应方程式

HRID 594678 的结构方程式

REACTANTS

反应物

2
结构：NCc1ccc(OC(F)(F)F)cc1
HCID571846

4-(Trifluoromethoxy)benzylamine

C8H8F3NO

结构：O=Cc1cccc2c1OCCO2
HCID2795033

2,3-dihydro-1,4-benzodioxine-5-carbaldehyde

C9H8O3

PRODUCTS

生成物

1
结构：O=C1C(O)CC(c2cccc3c2OCCO3)N1Cc1ccc(OC(F)(F)F)cc1
HCID69085698

未命名化合物

PROCEDURE

实验过程

Prepared according to the described general procedures 10A2 (GP10A2), 10B (GP10B) and 10F (GP10F) using commercially available (4-(trifluoromethoxy)phenyl)methanamine and commercially available 2,3-dihydrobenzo[b][1,4]dioxine-5-carbaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.79 min.; [M+H]+: 409.94 g/mol.

WORKUP

后处理

  1. customPrepared
  2. customSubsequent purification by preparative HPLC
  3. customafforded the target compound