huagongshe.com
HRID594691

反应详情

EQUATION

反应方程式

HRID 594691 的结构方程式

REACTANTS

反应物

2
结构：Cc1nc(-c2cccc(C=O)c2)cs1
HCID7127782

3-(2-methyl-1,3-thiazol-4-yl)benzaldehyde

C11H9NOS

结构：COC(=O)C(C)CC(N)c1c(OC)ccnc1OC
HCID69085168

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccnc(OC)c1C1CC(C)C(=O)N1Cc1cccc(-c2csc(C)n2)c1
HCID69083488

未命名化合物

PROCEDURE

实验过程

Prepared according to the described general procedure 2 (GP2) by reaction of methyl 4-amino-4-(2,4-dimethoxypyridin-3-yl)-2-methylbutanoate with commercially available 3-(2-methylthiazol-4-yl)benzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.73 min.; [M+H]+: 424.03 g/mol.

WORKUP

后处理

  1. customPrepared
  2. customSubsequent purification by preparative HPLC
  3. customafforded the target compound