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HRID594697

反应详情

EQUATION

反应方程式

HRID 594697 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(-c2nc(C=O)cs2)cc1
HCID14023571

2-(4-Methylphenyl)-1,3-thiazole-4-carbaldehyde

C11H9NOS

结构：CCOC(=O)C(C)CC(N)c1c(F)cccc1OC
HCID69085707

Benzenebutanoic acid, γ-amino-2-fluoro-6-methoxy-α-methyl-, ethyl ester

C14H20FNO3

PRODUCTS

生成物

1
结构：COc1cccc(F)c1C1CC(C)C(=O)N1Cc1csc(-c2ccc(C)cc2)n1
HCID69081676

未命名化合物

PROCEDURE

实验过程

Prepared according to the described general procedure 2 (GP2) by reaction of ethyl 4-amino-4-(2-fluoro-6-methoxyphenyl)-2-methylbutanoate with commercially available 2-(p-tolyl)thiazole-4-carbaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.94 min.; [M+H]+: 411.02 g/mol.

WORKUP

后处理

  1. customPrepared
  2. customSubsequent purification by preparative HPLC
  3. customafforded the target compound