HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethoxy-6-fluorobenzaldehyde → HCID 86695669, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethoxy-6-fluorobenzaldehyde | HCID 3815894 | — |
| Reactant | 3-Fluoro-4-(trifluoromethoxy)benzylamine | HCID 17750674 | — |
| Product | HCID 86695669 | HCID 86695669 | — |
Reaction Steps
Prepared according to the described general procedures 10A2 (GP10A2), 10B (GP10B), 10F (GP10F), and 10I (GP10I) using commercially available (3-fluoro-4-(trifluoromethoxy)phenyl)methanamine and synthesized 2-ethoxy-6-fluorobenzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.93 min.; [M+H]+: 433.92 g/mol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242970B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-061b1067b6464141b1ffc53bfe142a46 |
| Source note | uspto-grants-2016_01 |