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HRID594761

反应详情

EQUATION

反应方程式

HRID 594761 的结构方程式

REACTANTS

反应物

2
结构：CCOc1cccc(F)c1C=O
HCID3815894

未命名化合物

结构：NCc1ccc(OC(F)(F)F)c(Cl)c1
HCID53414455

1-[3-Chloro-4-(trifluoromethoxy)phenyl]methanamine

C8H7ClF3NO

PRODUCTS

生成物

1
结构：CCOc1cccc(F)c1C1CC(Cl)C(=O)N1Cc1ccc(OC(F)(F)F)c(Cl)c1
HCID86695670

未命名化合物

PROCEDURE

实验过程

Prepared according to the described general procedures 10A2 (GP10A2), 10B (GP10B), 10F (GP10F), and 10D (GP10D) using commercially available (3-chloro-4-(trifluoromethoxy)phenyl)methanamine and synthesized 2-ethoxy-6-fluorobenzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=1.00 min.; [M+H]+: 465.77 g/mol.

WORKUP

后处理

  1. customPrepared
  2. customSubsequent purification by preparative HPLC
  3. customafforded the target compound