HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67112430, compound → HCID 43641970, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67112430 | HCID 67112430 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 43641970 | HCID 43641970 | — |
Reaction Steps
A solution of N-methyl-4-nitro-1H-pyrrole-2-carboxamide (75 mg, 0.44 mmol) in methanol was degassed and flushed with N2 (g). 10% Pd on activated carbon was added and the mixture degassed and flushed with N2 (g). H2 (g) was applied and the reaction mixture stirred at rt for 14 h. The resultant mixture was filtered through celite then concentrated in vacuo to afford 4-amino-N-methyl-1H-pyrrole-2-carboxamide as a green solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09242987B2 |
| Source dataset | uspto-grants-2016_01 |
| ORD ID | ord-5e6606411073421c9df5519998f472f7 |
| Source note | uspto-grants-2016_01 |