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HRID595092

反应详情

EQUATION

反应方程式

HRID 595092 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)Nc1nc2c(s1)C(=O)CC(C)C2
HCID4644134

N-(4,5,6,7-Tetrahydro-5-methyl-7-oxo-2-benzothiazolyl)acetamide

C10H12N2O2S

结构：O=C(Cl)c1ccc(F)nc1
HCID14623602

6-Fluoropyridine-3-carbonyl chloride

C6H3ClFNO

PRODUCTS

生成物

1
结构：CC(=O)Nc1nc2c(s1)C(=O)C(C(=O)c1ccc(F)nc1)C(C)C2
HCID86664611

未命名化合物

PROCEDURE

实验过程

A-16 is prepared via general procedure A1 starting from 2-fluoropyridine-5-carbonyl chloride (4.27 g, 26.8 mmol) and N-(5-methyl-7-oxo-4,5,6,7-tetrahydro-benzothiazol-2-yl)-acetamide (A-06) (5.00 g, 22.3 mmol). Yield: 6.20 g. HPLC-MS: tR=0.93 min, (M+H)+=348.

WORKUP

后处理

  1. customA-16 is prepared via general procedure A1