HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 12251285, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 12251284 | HCID 12251284 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12251285 | HCID 12251285 | — |
Reaction Steps
A 3',4'-dihydrospiro[cyclohexane-1,1'(2'H)-naphthalen]-4-one (r) produced in step (10) has its 4-keto function reduced, e.g., by mixing said compound in a solvent such as ethanol with sodium borohydride at moderate (room) temperature for from about 3 to about 8 hours, to produce a corresponding 3',4'-dihydrospiro[cyclohexane-1,1'(2H)naphthalen]-4-ol (s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04010201 |
| Source dataset | uspto-grants-1977_03 |
| ORD ID | ord-4040aa4959ff4e4f84c95bd5a0c2c795 |
| Source note | uspto-grants-1977_03 |