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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 596354Generated: October 29, 2026

2-Hydroxyacetohydrazide → HCID 19865793, compound

https://huagongshe.com/reaction/596354

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-HydroxyacetohydrazideHCID 350536—
ReactantHCID 19865818HCID 19865818—
Solvent1-ButanolHCID 263—
ProductHCID 19865793HCID 19865793—

Reaction Steps

In the manner given in Example 1, a solution of 1,3-dihydro-7-trifluoromethyl-5-(o-chlorophenyl)-2H-1,4-benzodiazepine-2-thione and hydroxyacetic acid hydrazide in n-butyl alcohol is refluxed to give 8-trifluoromethyl-1-(hydroxymethyl)-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine. Preparation 5 1-(Hydroxymethyl)-6-(o-chlorophenyl)-4H-s-triazolo[4,3-a][1,4]benzodiazepine

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04010177
Source datasetuspto-grants-1977_03
ORD IDord-bea704b51bad49259827afd5f49018a8
Source noteuspto-grants-1977_03